Ammonium Molybdate Solution (I) Add 2 ml of conc. H2SO4 (Sulphuric acid) carefully to 100 ml of demineralised water. (ii) Dissolve 25 gms of ammonium molybdate in 100 cc of demineralised water. Mix (i) and (ii) and make up the volume to 333 ml. 10% Oxalic Acid: Dissolve 25 gm of oxalic acid in 250 ml of demineralised water. A.N.S. Solution : i)Take 3.5 gm of sodium sulphite in a dry mortar and add 0.375 gm 1- Amino - 2 naphthol 4- sulphonic acid (A.N.S.) to it and grind well. Mix this in 50 ml of demineralised water ii)Add 22.5 of sodium sulphite to 200 ml demineralised water and mix well. Mix solutions (i) and (ii) . Take 50 ml water sample in a 100 ml beaker. Add 2 ml of Ammonium molydate solution prepared (as in 6.1) wait for 2 minutes . Add 4 ml of oxalic acid (6.2) and 1 ml of A.N.S. solution (6.3) without any time gap. Without any time gap. Wait for 4 minutes. The developed blue colour is matched or measured with the known value of low ...
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